341 lines
10 KiB
JSON
341 lines
10 KiB
JSON
{
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"cues": {
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"cue #": [
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1,
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9
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],
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"timestamp": [
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1667219342.05907,
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1667230280.2648277,
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1667230870.4126155,
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1667231244.7715194,
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1667231274.5002868,
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1667233422.1033566,
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1667234899.3792205,
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1667237976.1180177,
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1667238545.023338,
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1667238650.7824838,
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1667239560.3921096,
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1667220435.018817,
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1667247443.2248201,
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1667247469.6818917,
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1667255882.524956,
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1667255960.2140675,
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1667256037.315233,
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1667256059.81643,
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1667256181.6962314,
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1667256187.704754,
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1667258176.372912,
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1667274351.2824874,
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1667221421.3997478,
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1667274377.580271,
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1667277047.9328628,
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1667277813.004019,
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1667277852.243938,
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1667277870.5923216,
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1667279779.7239056,
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1667221617.2863898,
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1667221634.9071724,
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1667224689.0929015,
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1667225839.6906874,
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1667225936.7263315,
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1667226292.7996562
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],
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"comment": [
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"30 ml/min\n",
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"7.5 ml/min since cell 3",
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"37.5 ml/min for 5s then again 7.5 ml/min",
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"37.5 ml/min for 5s then again 7.5 ml/min",
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"7.5 ml/min",
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"0 ml/min",
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"7.5 ml/min",
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"15 ml/min",
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"7.5 ml/min",
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"0 ml/min",
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"7.5 ml/min",
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"0 ml/min 30s before",
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"30 ml/min",
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"7.5 ml/min",
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"30 ml/min",
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"0 ml/min (when failure is happening)",
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"30 ml/min",
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"7.5 ml/min",
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"30 ml/min",
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"0 ml/min (too late)",
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"7.5 ml/min",
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"30 ml/min",
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"7.5 ml/min",
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"7.5 ml/min",
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"30 ml/min then immediatly 7.5 ml/min",
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"30 ml/min",
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"0 ml/min",
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"7.5 ml/min",
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"10 ml/min",
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"30 ml/min",
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"7.5 ml/min",
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"40 ml/min 2min ago",
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"100 ml/min",
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"30 ml/min",
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"300 ml/min"
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]
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},
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"EC_folder": "I:\\01_imaging_at_TOMCAT_Robert\\02_EC_data_for_image_data",
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"samples": {
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"3": {
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"pre-damage": "T_3_scan_02",
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"post-damage": "T_3_scan_03",
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"comment": "test sample: beam damage tests. Series of 10 s exposures (7) + 1 60s exposure + 10 s before seeing decrease of EC-performance"
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},
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"3II": {
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"ec_lab_names": [
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"3b"
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],
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"ec_lab_files": [
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"cell_3b_01_PEIS_C01.mgr",
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"cell_3b_01_PEIS_C01.mpr",
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"cell_3b_02_GEIS_C01.mgr",
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"cell_3b_02_GEIS_C01.mpr",
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"cell_3b_DUSB0_C01.sta"
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],
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"no_gas_no_water": "T_3b_scan_02",
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"gas_no_water": "T_3b_scan_03",
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"gas_water": "T_3b_scan_04",
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"operando": [
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"T_3b_scan_05",
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"T_3b_scan_06",
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"T_3b_scan_07"
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],
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"main EC condition": "pot. stat. 3.5V"
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},
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"3III": {
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"ec_lab_names": [
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"3iii"
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],
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"ec_lab_files": [
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"cell_3iii_01_PEIS_C01.mgr",
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"cell_3iii_01_PEIS_C01.mpr",
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"cell_3iii_02_GEIS_C01.mgr",
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"cell_3iii_02_GEIS_C01.mpr",
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"cell_3iii_DUSB0_C01.sta"
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],
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"no_gas_no_water": "T_3III_01",
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"gas_no_water": "T_3III_scan_02",
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"gas_water": "T_3III_scan_03",
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"operando": [
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"T_3III_scan_04",
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"T_3III_scan_05"
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],
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"comment": "cathode flow field from former cell 6 due to capillaries ripped off",
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"main EC condition": "pot. stat. 3V"
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},
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"4": {
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"ec_lab_names": [
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"4"
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],
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"ec_lab_files": [
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"cell_4_scan1.mps",
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"cell_4_scan1_01_PEIS_C01.mgr",
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"cell_4_scan1_01_PEIS_C01.mpr",
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"cell_4_scan1_02_GEIS_C01.mgr",
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"cell_4_scan1_02_GEIS_C01.mpr",
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"cell_4_scan1_DUSB0_C01.sta"
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],
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"no_gas_no_water": "n.a.",
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"gas_no_water": "n.a.",
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"gas_water": "T_4_scan_01",
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"operando": [
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"T_4_scan_02",
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"T_4_scan_03"
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],
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"main EC condition": "galv. stat. 3mA"
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},
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"4II": {
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"ec_lab_names": [
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"4ii",
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"4iib"
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],
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"ec_lab_files": [
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"cell_4iib_01_PEIS_C01.mgr",
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"cell_4iib_01_PEIS_C01.mpr",
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"cell_4iib_02_GEIS_C01.mgr",
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"cell_4iib_02_GEIS_C01.mpr",
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"cell_4iib_DUSB0_C01.sta"
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],
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"no_gas_no_water": "T_4_scan_01",
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"gas_no_water": "T_4_scan_02",
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"gas_water": "T_4_scan_03",
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"operando": [
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"T_4_scan_05"
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],
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"comment": "operando scan 4 cancelled within first minute to fix dangerously moving tubing",
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"main EC condition": "current ramp up"
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},
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"5": {
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"ec_lab_names": [
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"5"
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],
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"ec_lab_files": [
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"cell_5_scan1.mps",
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"cell_5_scan1b.mps",
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"cell_5_scan1b_01_PEIS_C01.mgr",
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"cell_5_scan1b_01_PEIS_C01.mpr",
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"cell_5_scan1b_02_GEIS_C01.mgr",
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"cell_5_scan1b_02_GEIS_C01.mpr",
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"cell_5_scan1b_DUSB0_C01.sta",
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"cell_5_scan1_01_PEIS_C01.mgr",
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"cell_5_scan1_01_PEIS_C01.mpr",
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"cell_5_scan1_02_GEIS_C01.mgr",
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"cell_5_scan1_02_GEIS_C01.mpr",
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"cell_5_scan1_DUSB0_C01.sta"
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],
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"no_gas_no_water": "T_5_scan_02",
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"gas_no_water": "T_5_scan_03",
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"gas_water": "T_5_scan_04",
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"operando": [
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"T_5_scan_05",
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"T_5_scan_06",
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"T_5_scan_07"
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],
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"main EC condition": "galv. stat. initially 3mA, ramped up to 20mA"
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},
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"5II": {
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"ec_lab_names": [
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"5ii"
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],
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"ec_lab_files": [
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"cell_5ii_01_PEIS_C01.mgr",
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"cell_5ii_01_PEIS_C01.mpr",
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"cell_5ii_02_GEIS_C01.mgr",
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"cell_5ii_02_GEIS_C01.mpr",
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"cell_5ii_DUSB0_C01.sta"
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],
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"no_gas_no_water": "T_5II_scan_01",
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"gas_no_water": "T_5II_scan_02",
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"gas_water": "T_5II_scan_03",
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"operando": [
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"T_5II_scan_04"
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],
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"comment": "flooded rotation stage and probably unreliable EC-measurements",
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"main EC condition": "pot. stat. 3.5V"
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},
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"6": {
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"ec_lab_names": [
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"6",
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"6b"
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],
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"ec_lab_files": [
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"cell_6_01_PEIS_C01.mgr",
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"cell_6_01_PEIS_C01.mpr",
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"cell_6_02_GEIS_C01.mgr",
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"cell_6_02_GEIS_C01.mpr",
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"cell_6_DUSB0_C01.sta",
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"cell_6b_01_PEIS_C01.mgr",
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"cell_6b_01_PEIS_C01.mpr",
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"cell_6b_02_GEIS_C01.mgr",
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"cell_6b_02_GEIS_C01.mpr",
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"cell_6b_DUSB0_C01.sta"
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],
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"no_gas_no_water": "T_6_scan_01",
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"gas_no_water": "T_6_scan_02",
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"gas_water": "T_6_scan_03",
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"operando": [
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"T_6_scan_04",
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"T_6_scan_05",
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"T_6_scan_06"
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],
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"main EC condition": "galv. stat. 5mA"
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},
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"7x": {
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"ec_lab_names": [
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"7x"
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],
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"ec_lab_files": [
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"cell_7x_01_PEIS_C01.mgr",
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"cell_7x_01_PEIS_C01.mpr",
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"cell_7x_02_GEIS_C01.mgr",
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"cell_7x_02_GEIS_C01.mpr",
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"cell_7x_DUSB0_C01.sta"
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],
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"no_gas_no_water": "T_7x_scan_01",
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"gas_no_water": "T_7x_scan_02",
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"gas_water": "T_7x_scan_03",
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"operando": [
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"T_7x_scan_04"
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],
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"comment": "pinched GDL, gas flow at 10ml/min",
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"main EC condition": "galv. stat. 5mA"
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},
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"8x": {
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"ec_lab_names": [
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"8x"
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],
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"ec_lab_files": [
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"cell_8x_01_PEIS_C01.mgr",
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"cell_8x_01_PEIS_C01.mpr",
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"cell_8x_02_GEIS_C01.mgr",
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"cell_8x_02_GEIS_C01.mpr",
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"cell_8x_DUSB0_C01.sta"
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],
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"no_gas_no_water": "T_8x_scan_01",
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"gas_no_water": "T_8x_scan_02",
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"gas_water": "T_8x_scan_03",
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"operando": [
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"T_8x_scan_04"
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],
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"comment": "pinched GDL",
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"main EC condition": "current ramp up"
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},
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"1": {
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"test 1": "T_1_scan_01",
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"test 2": "T_1_scan_02",
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"dry reference": "T_1_scan_03",
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"dynamic scan running water": "T_1_scan_04",
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"dynamic scan gas+water": "T_1_scan_05",
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"comment": "test sample: beam setup and water transport without electrochemistry"
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}
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},
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"test_samples": {
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"1": {
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"comment": "testing setup and without echem, e.g. operando with gas (see logbook)"
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},
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"2": {
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"comment": "tests, unfortunately gas not connected"
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},
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"3": {
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"comment": "beam damage tests"
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}
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}
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} |